Metabolites from the Plant Endophytic Fungus Aspergillus sp. CPCC 400735 and Their Anti-HIV Activities

  • J Nat Prod. 2017 Oct 27;80(10):2595-2601. doi: 10.1021/acs.jnatprod.6b00878.
Xu Pang  1 Jian-Yuan Zhao  1 Xiao-Mei Fang  1 Tao Zhang  1 De-Wu Zhang  1 Hong-Yu Liu  1 Jing Su  1 Shan Cen  1 Li-Yan Yu  1
Affiliations
  • 1. Institute of Medicinal Biotechnology, Academy of Medical Science & Peking Union Medical College , Beijing 100050, China.
Abstract

Thirty-three metabolites including five phenalenone derivatives (1-5), seven cytochalasins (6-12), thirteen butenolides (13-25), and eight phenyl derivatives (26-33) were isolated from Aspergillus sp. CPCC 400735 cultured on rice. The structures of all compounds were elucidated by NMR, MS, and CD experiments, of which 1-5 (asperphenalenones A-E), 6 (aspochalasin R), and 13 (aspulvinone R) were identified as new compounds. Specifically, asperphenalenones A-E (1-5) represent an unusual structure composed of a linear diterpene derivative linked to a phenalenone derivative via a C-C bond. Compounds 1, 4, 10, and 26 exhibited anti-HIV activity with IC50 values of 4.5, 2.4, 9.2, and 6.6 μM, respectively (lamivudine 0.1 μM; efavirenz, 0.4 × 10-3 μM).